Chemical constituents of extracted oil from the nut of Pistacia atlantica kurdica (dried and fresh samples) - which grows in some regions of Kurdistan province in Iran - were extracted by using soxhlet method and analyzed by gas chromatography mass spectrometry. The main goal of this study was qualitative analysis of extracted compounds and optimization of extraction conditions. At three extraction times (7h, 11h and 13h) and with two solvents (n-hexane and methanol), soxhlet extractions were carried out. Extraction time and type of solvents were selected as two important factors. A general full factorial design with selected factors was used. The study reveals that n-hexane extracted more yield than methanol. The highest yield obtained with n-hexane, was 33.59%; while the highest yield obtained by methanol was 3.85%. The results show that when extraction is done by n-hexane, by increasing the extraction time up to 11h, the mass yield percent was also increased. The obtained chromatograms were showed that by increasing the extraction time up to 13h, the main extracted compounds were maintained but compounds with low quantities have been eliminated. The main compounds identified were alpha-pinene, decane, dodecane, tetradecane, hexadecane, palmitic acid, oleic acid and linoleic acid ester. The main identified compounds were nearly similar to dried and fresh samples. This study can be considered as the firs report on the chemical compounds of extracted oil from nut of Pistacia atlantica kurdica in studied region.
| Published in | Science Journal of Analytical Chemistry (Volume 3, Issue 6) |
| DOI | 10.11648/j.sjac.20150306.17 |
| Page(s) | 122-126 |
| Creative Commons |
This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited. |
| Copyright |
Copyright © The Author(s), 2015. Published by Science Publishing Group |
Pistacia Atlantica Kurdica, Soxhlet, Oil Extraction
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APA Style
Atena Ghaderi, Bahram Ebrahimi. (2015). Soxhlet Extraction and Gas Chromatography Mass Spectrometry Analysis of Extracted Oil from Pistacia Atlantica Kurdica Nuts and Optimization of Process Using Factorial Design of Experiments. Science Journal of Analytical Chemistry, 3(6), 122-126. https://doi.org/10.11648/j.sjac.20150306.17
ACS Style
Atena Ghaderi; Bahram Ebrahimi. Soxhlet Extraction and Gas Chromatography Mass Spectrometry Analysis of Extracted Oil from Pistacia Atlantica Kurdica Nuts and Optimization of Process Using Factorial Design of Experiments. Sci. J. Anal. Chem. 2015, 3(6), 122-126. doi: 10.11648/j.sjac.20150306.17
AMA Style
Atena Ghaderi, Bahram Ebrahimi. Soxhlet Extraction and Gas Chromatography Mass Spectrometry Analysis of Extracted Oil from Pistacia Atlantica Kurdica Nuts and Optimization of Process Using Factorial Design of Experiments. Sci J Anal Chem. 2015;3(6):122-126. doi: 10.11648/j.sjac.20150306.17
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Download@article{10.11648/j.sjac.20150306.17,
author = {Atena Ghaderi and Bahram Ebrahimi},
title = {Soxhlet Extraction and Gas Chromatography Mass Spectrometry Analysis of Extracted Oil from Pistacia Atlantica Kurdica Nuts and Optimization of Process Using Factorial Design of Experiments},
journal = {Science Journal of Analytical Chemistry},
volume = {3},
number = {6},
pages = {122-126},
doi = {10.11648/j.sjac.20150306.17},
url = {https://doi.org/10.11648/j.sjac.20150306.17},
eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.sjac.20150306.17},
abstract = {Chemical constituents of extracted oil from the nut of Pistacia atlantica kurdica (dried and fresh samples) - which grows in some regions of Kurdistan province in Iran - were extracted by using soxhlet method and analyzed by gas chromatography mass spectrometry. The main goal of this study was qualitative analysis of extracted compounds and optimization of extraction conditions. At three extraction times (7h, 11h and 13h) and with two solvents (n-hexane and methanol), soxhlet extractions were carried out. Extraction time and type of solvents were selected as two important factors. A general full factorial design with selected factors was used. The study reveals that n-hexane extracted more yield than methanol. The highest yield obtained with n-hexane, was 33.59%; while the highest yield obtained by methanol was 3.85%. The results show that when extraction is done by n-hexane, by increasing the extraction time up to 11h, the mass yield percent was also increased. The obtained chromatograms were showed that by increasing the extraction time up to 13h, the main extracted compounds were maintained but compounds with low quantities have been eliminated. The main compounds identified were alpha-pinene, decane, dodecane, tetradecane, hexadecane, palmitic acid, oleic acid and linoleic acid ester. The main identified compounds were nearly similar to dried and fresh samples. This study can be considered as the firs report on the chemical compounds of extracted oil from nut of Pistacia atlantica kurdica in studied region.},
year = {2015}
}
TY - JOUR T1 - Soxhlet Extraction and Gas Chromatography Mass Spectrometry Analysis of Extracted Oil from Pistacia Atlantica Kurdica Nuts and Optimization of Process Using Factorial Design of Experiments AU - Atena Ghaderi AU - Bahram Ebrahimi Y1 - 2015/12/16 PY - 2015 N1 - https://doi.org/10.11648/j.sjac.20150306.17 DO - 10.11648/j.sjac.20150306.17 T2 - Science Journal of Analytical Chemistry JF - Science Journal of Analytical Chemistry JO - Science Journal of Analytical Chemistry SP - 122 EP - 126 PB - Science Publishing Group SN - 2376-8053 UR - https://doi.org/10.11648/j.sjac.20150306.17 AB - Chemical constituents of extracted oil from the nut of Pistacia atlantica kurdica (dried and fresh samples) - which grows in some regions of Kurdistan province in Iran - were extracted by using soxhlet method and analyzed by gas chromatography mass spectrometry. The main goal of this study was qualitative analysis of extracted compounds and optimization of extraction conditions. At three extraction times (7h, 11h and 13h) and with two solvents (n-hexane and methanol), soxhlet extractions were carried out. Extraction time and type of solvents were selected as two important factors. A general full factorial design with selected factors was used. The study reveals that n-hexane extracted more yield than methanol. The highest yield obtained with n-hexane, was 33.59%; while the highest yield obtained by methanol was 3.85%. The results show that when extraction is done by n-hexane, by increasing the extraction time up to 11h, the mass yield percent was also increased. The obtained chromatograms were showed that by increasing the extraction time up to 13h, the main extracted compounds were maintained but compounds with low quantities have been eliminated. The main compounds identified were alpha-pinene, decane, dodecane, tetradecane, hexadecane, palmitic acid, oleic acid and linoleic acid ester. The main identified compounds were nearly similar to dried and fresh samples. This study can be considered as the firs report on the chemical compounds of extracted oil from nut of Pistacia atlantica kurdica in studied region. VL - 3 IS - 6 ER -
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