Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer

Y. Yildiz; M. Dasgupta

doi:doi:10.11648/j.sjac.20160403.11

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Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer

Y. Yildiz, M. Dasgupta

Published in Science Journal of Analytical Chemistry (Volume 4, Issue 3)

Received: 19 March 2016 Accepted: 7 April 2016 Published: 27 April 2016

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Abstract

Tricalcium Phosphate Anhydrous Powder typically contains 300 to 400 mg/Kg (w/w) of aluminum. This level can be determined utilizing AAS and standard based on known standards. In this study, we have determined the amount of aluminum metal present in sample of Tricalcium Phosphate Anhydrous Powder using Atomic Absorption Spectrophotometer (AAS). The method has high precision and accuracy. The results of aluminum determinations obtained by employment of N2O-C2H2 flame AAS methods. Great care is necessary for preparation of the blank. The need to subtract blank with standard calibration curve this was done automatically. The accuracy was checked with recovery test of aluminum added to the sample before analysis. With employment of AAS method 98.5% and 99.0% of added aluminum was recovered. The detection limit for the determination of Al was 0.5 mg/Kg and results meet the requirements.

Published in	Science Journal of Analytical Chemistry (Volume 4, Issue 3)
DOI	10.11648/j.sjac.20160403.11
Page(s)	22-25
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2016. Published by Science Publishing Group

Keywords

Tricalcium Phosphate, Aluminum Determination, Flame Atomic Absorption Spectrophotometer

References

[1]	Ober, JA, Phosphate Rocks; U.S. Geological Survey Mineral Information.
[2]	Ahmed, M. J. and J. Hossan, 1995. Spectrophotometric determination of aluminum by morin. Talanta, 42(8): 1135-1142.
[3]	Huseyinli, A. A., R. Aliyeva, S. Haciyeva and T. Guray, 2009. Spectrophotometric determination of aluminum and indium with 2,2,3,4-tetrahydroxy-3,5-disulphoazobenzene. Journal of Hazardous Materials, 163: 1001-1007.
[4]	Francisco, B. A., L. S. Caldas, D. M. Brum and R. J. Cassella, 2010. Novel spectrophoto metricmethod for the determination of aluminum in soda drinks packed in cans and plastic bottles. Journal of Hazardous Materials, 181: 485-490.
[5]	Honorato, R. S., J. M. T. Carnerio and E. A. G. Zagatto, 2001. Spectrophotometric flow-batch determination of aluminum in plant tissues exploiting a feedback mechanism. Analytical Chimica Acta, 441:309-315.
[6]	Bulut, V. N., D. Arslan, D. Ozdes, M. Soylak and M. Tufekci, 2010. Preconcentration, separation and spectrophotometric determination of aluminum (III) in water samples and dialysis concentrates at trace levels with 8-hydroxyquinoline-cobalt(II) coprecipitation system. 182: 331-336.
[7]	Burguera, J. L., M. Burguera, C. Rondon, P. Carrero, M. R. Brunetto and Y. Petitde Pena, 2000. Determination of beryllium in natural and waste waters using on-line flow-injection preconcentration by precipitation: dissolution for electrothermal atomic absorption spectrometry. Talanta, 52: 27-37.

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APA Style

Y. Yildiz, M. Dasgupta. (2016). Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer. Science Journal of Analytical Chemistry, 4(3), 22-25. https://doi.org/10.11648/j.sjac.20160403.11

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ACS Style

Y. Yildiz; M. Dasgupta. Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer. Sci. J. Anal. Chem. 2016, 4(3), 22-25. doi: 10.11648/j.sjac.20160403.11

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AMA Style

Y. Yildiz, M. Dasgupta. Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer. Sci J Anal Chem. 2016;4(3):22-25. doi: 10.11648/j.sjac.20160403.11

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@article{10.11648/j.sjac.20160403.11,
  author = {Y. Yildiz and M. Dasgupta},
  title = {Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer},
  journal = {Science Journal of Analytical Chemistry},
  volume = {4},
  number = {3},
  pages = {22-25},
  doi = {10.11648/j.sjac.20160403.11},
  url = {https://doi.org/10.11648/j.sjac.20160403.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.sjac.20160403.11},
  abstract = {Tricalcium Phosphate Anhydrous Powder typically contains 300 to 400 mg/Kg (w/w) of aluminum. This level can be determined utilizing AAS and standard based on known standards. In this study, we have determined the amount of aluminum metal present in sample of Tricalcium Phosphate Anhydrous Powder using Atomic Absorption Spectrophotometer (AAS). The method has high precision and accuracy. The results of aluminum determinations obtained by employment of N2O-C2H2 flame AAS methods. Great care is necessary for preparation of the blank. The need to subtract blank with standard calibration curve this was done automatically. The accuracy was checked with recovery test of aluminum added to the sample before analysis. With employment of AAS method 98.5% and 99.0% of added aluminum was recovered. The detection limit for the determination of Al was 0.5 mg/Kg and results meet the requirements.},
 year = {2016}
}

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TY  - JOUR
T1  - Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer
AU  - Y. Yildiz
AU  - M. Dasgupta
Y1  - 2016/04/27
PY  - 2016
N1  - https://doi.org/10.11648/j.sjac.20160403.11
DO  - 10.11648/j.sjac.20160403.11
T2  - Science Journal of Analytical Chemistry
JF  - Science Journal of Analytical Chemistry
JO  - Science Journal of Analytical Chemistry
SP  - 22
EP  - 25
PB  - Science Publishing Group
SN  - 2376-8053
UR  - https://doi.org/10.11648/j.sjac.20160403.11
AB  - Tricalcium Phosphate Anhydrous Powder typically contains 300 to 400 mg/Kg (w/w) of aluminum. This level can be determined utilizing AAS and standard based on known standards. In this study, we have determined the amount of aluminum metal present in sample of Tricalcium Phosphate Anhydrous Powder using Atomic Absorption Spectrophotometer (AAS). The method has high precision and accuracy. The results of aluminum determinations obtained by employment of N2O-C2H2 flame AAS methods. Great care is necessary for preparation of the blank. The need to subtract blank with standard calibration curve this was done automatically. The accuracy was checked with recovery test of aluminum added to the sample before analysis. With employment of AAS method 98.5% and 99.0% of added aluminum was recovered. The detection limit for the determination of Al was 0.5 mg/Kg and results meet the requirements.
VL  - 4
IS  - 3
ER  -

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Author Information

Y. Yildiz

Complete Analysis Laboratories, Analytical Research Department, Parsippany, NJ, USA
M. Dasgupta

Complete Analysis Laboratories, Analytical Research Department, Parsippany, NJ, USA

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APA Style

Y. Yildiz, M. Dasgupta. (2016). Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer. Science Journal of Analytical Chemistry, 4(3), 22-25. https://doi.org/10.11648/j.sjac.20160403.11

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ACS Style

Y. Yildiz; M. Dasgupta. Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer. Sci. J. Anal. Chem. 2016, 4(3), 22-25. doi: 10.11648/j.sjac.20160403.11

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AMA Style

Y. Yildiz, M. Dasgupta. Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer. Sci J Anal Chem. 2016;4(3):22-25. doi: 10.11648/j.sjac.20160403.11

Copy | Download

@article{10.11648/j.sjac.20160403.11,
  author = {Y. Yildiz and M. Dasgupta},
  title = {Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer},
  journal = {Science Journal of Analytical Chemistry},
  volume = {4},
  number = {3},
  pages = {22-25},
  doi = {10.11648/j.sjac.20160403.11},
  url = {https://doi.org/10.11648/j.sjac.20160403.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.sjac.20160403.11},
  abstract = {Tricalcium Phosphate Anhydrous Powder typically contains 300 to 400 mg/Kg (w/w) of aluminum. This level can be determined utilizing AAS and standard based on known standards. In this study, we have determined the amount of aluminum metal present in sample of Tricalcium Phosphate Anhydrous Powder using Atomic Absorption Spectrophotometer (AAS). The method has high precision and accuracy. The results of aluminum determinations obtained by employment of N2O-C2H2 flame AAS methods. Great care is necessary for preparation of the blank. The need to subtract blank with standard calibration curve this was done automatically. The accuracy was checked with recovery test of aluminum added to the sample before analysis. With employment of AAS method 98.5% and 99.0% of added aluminum was recovered. The detection limit for the determination of Al was 0.5 mg/Kg and results meet the requirements.},
 year = {2016}
}

Copy | Download

TY  - JOUR
T1  - Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer
AU  - Y. Yildiz
AU  - M. Dasgupta
Y1  - 2016/04/27
PY  - 2016
N1  - https://doi.org/10.11648/j.sjac.20160403.11
DO  - 10.11648/j.sjac.20160403.11
T2  - Science Journal of Analytical Chemistry
JF  - Science Journal of Analytical Chemistry
JO  - Science Journal of Analytical Chemistry
SP  - 22
EP  - 25
PB  - Science Publishing Group
SN  - 2376-8053
UR  - https://doi.org/10.11648/j.sjac.20160403.11
AB  - Tricalcium Phosphate Anhydrous Powder typically contains 300 to 400 mg/Kg (w/w) of aluminum. This level can be determined utilizing AAS and standard based on known standards. In this study, we have determined the amount of aluminum metal present in sample of Tricalcium Phosphate Anhydrous Powder using Atomic Absorption Spectrophotometer (AAS). The method has high precision and accuracy. The results of aluminum determinations obtained by employment of N2O-C2H2 flame AAS methods. Great care is necessary for preparation of the blank. The need to subtract blank with standard calibration curve this was done automatically. The accuracy was checked with recovery test of aluminum added to the sample before analysis. With employment of AAS method 98.5% and 99.0% of added aluminum was recovered. The detection limit for the determination of Al was 0.5 mg/Kg and results meet the requirements.
VL  - 4
IS  - 3
ER  -

Copy | Download