Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry

Almojtaba Abd Alkhalig Ahmed Bakheet; Xiashi Zhu

doi:doi:10.11648/j.sjac.20170506.17

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Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry

Almojtaba Abd Alkhalig Ahmed Bakheet, Xiashi Zhu

Published in Science Journal of Analytical Chemistry (Volume 5, Issue 6)

Received: 15 November 2017 Accepted: 25 November 2017 Published: 2 January 2018

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Abstract

Magnetic solid phase extraction (MSPE) accompanied with fluorescence spectrophotometry using Poly (ionic liquid) immobilized magnetic nanoparticles (PIL-MNPs) as sorbent was introduced for Congo red analysis in food. Poly (1-vinyl-3-butylimidazolium) bromide immobilized (MNPs) were prepared through co-polymerization of 1-vinyl-3-hexylimidazolium-based ionic liquid and vinyl-modified magnetic particles. Some of different types of parameters, such as pH value, adsorption temperature and time, sample volume, eluent type, were studied. Under the optimum conditions, the preconcentration factor for AR was 27. The linear range, detection limit (DL), correlation coefficient (R) and relative standard deviation (RSD) were found to be 0.10-9.00μg/mL, 5.2μg/L, 0.9987 and 3.10% (n=3, c=4.00μg/mL). This method had been successfully applied to the separation / analysis of Congo red in real samples.

Published in	Science Journal of Analytical Chemistry (Volume 5, Issue 6)
DOI	10.11648/j.sjac.20170506.17
Page(s)	113-118
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2018. Published by Science Publishing Group

Keywords

Congo Red, Poly (Ionic Liquid) Magnetic Nanoparticles, Magnetic Solid-Phase Extraction, Fluorescence Spectrophotometry

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APA Style

Almojtaba Abd Alkhalig Ahmed Bakheet, Xiashi Zhu. (2018). Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry. Science Journal of Analytical Chemistry, 5(6), 113-118. https://doi.org/10.11648/j.sjac.20170506.17

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ACS Style

Almojtaba Abd Alkhalig Ahmed Bakheet; Xiashi Zhu. Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry. Sci. J. Anal. Chem. 2018, 5(6), 113-118. doi: 10.11648/j.sjac.20170506.17

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AMA Style

Almojtaba Abd Alkhalig Ahmed Bakheet, Xiashi Zhu. Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry. Sci J Anal Chem. 2018;5(6):113-118. doi: 10.11648/j.sjac.20170506.17

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@article{10.11648/j.sjac.20170506.17,
  author = {Almojtaba Abd Alkhalig Ahmed Bakheet and Xiashi Zhu},
  title = {Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry},
  journal = {Science Journal of Analytical Chemistry},
  volume = {5},
  number = {6},
  pages = {113-118},
  doi = {10.11648/j.sjac.20170506.17},
  url = {https://doi.org/10.11648/j.sjac.20170506.17},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.sjac.20170506.17},
  abstract = {Magnetic solid phase extraction (MSPE) accompanied with fluorescence spectrophotometry using Poly (ionic liquid) immobilized magnetic nanoparticles (PIL-MNPs) as sorbent was introduced for Congo red analysis in food. Poly (1-vinyl-3-butylimidazolium) bromide immobilized (MNPs) were prepared through co-polymerization of 1-vinyl-3-hexylimidazolium-based ionic liquid and vinyl-modified magnetic particles. Some of different types of parameters, such as pH value, adsorption temperature and time, sample volume, eluent type, were studied. Under the optimum conditions, the preconcentration factor for AR was 27. The linear range, detection limit (DL), correlation coefficient (R) and relative standard deviation (RSD) were found to be 0.10-9.00μg/mL, 5.2μg/L, 0.9987 and 3.10% (n=3, c=4.00μg/mL). This method had been successfully applied to the separation / analysis of Congo red in real samples.},
 year = {2018}
}

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TY  - JOUR
T1  - Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry
AU  - Almojtaba Abd Alkhalig Ahmed Bakheet
AU  - Xiashi Zhu
Y1  - 2018/01/02
PY  - 2018
N1  - https://doi.org/10.11648/j.sjac.20170506.17
DO  - 10.11648/j.sjac.20170506.17
T2  - Science Journal of Analytical Chemistry
JF  - Science Journal of Analytical Chemistry
JO  - Science Journal of Analytical Chemistry
SP  - 113
EP  - 118
PB  - Science Publishing Group
SN  - 2376-8053
UR  - https://doi.org/10.11648/j.sjac.20170506.17
AB  - Magnetic solid phase extraction (MSPE) accompanied with fluorescence spectrophotometry using Poly (ionic liquid) immobilized magnetic nanoparticles (PIL-MNPs) as sorbent was introduced for Congo red analysis in food. Poly (1-vinyl-3-butylimidazolium) bromide immobilized (MNPs) were prepared through co-polymerization of 1-vinyl-3-hexylimidazolium-based ionic liquid and vinyl-modified magnetic particles. Some of different types of parameters, such as pH value, adsorption temperature and time, sample volume, eluent type, were studied. Under the optimum conditions, the preconcentration factor for AR was 27. The linear range, detection limit (DL), correlation coefficient (R) and relative standard deviation (RSD) were found to be 0.10-9.00μg/mL, 5.2μg/L, 0.9987 and 3.10% (n=3, c=4.00μg/mL). This method had been successfully applied to the separation / analysis of Congo red in real samples.
VL  - 5
IS  - 6
ER  -

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Author Information

Almojtaba Abd Alkhalig Ahmed Bakheet

College of Chemistry & Chemical Engineering, Yangzhou University, Yangzhou, China
Xiashi Zhu

College of Chemistry & Chemical Engineering, Yangzhou University, Yangzhou, China

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APA Style

Almojtaba Abd Alkhalig Ahmed Bakheet, Xiashi Zhu. (2018). Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry. Science Journal of Analytical Chemistry, 5(6), 113-118. https://doi.org/10.11648/j.sjac.20170506.17

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ACS Style

Almojtaba Abd Alkhalig Ahmed Bakheet; Xiashi Zhu. Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry. Sci. J. Anal. Chem. 2018, 5(6), 113-118. doi: 10.11648/j.sjac.20170506.17

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AMA Style

Almojtaba Abd Alkhalig Ahmed Bakheet, Xiashi Zhu. Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry. Sci J Anal Chem. 2018;5(6):113-118. doi: 10.11648/j.sjac.20170506.17

Copy | Download

@article{10.11648/j.sjac.20170506.17,
  author = {Almojtaba Abd Alkhalig Ahmed Bakheet and Xiashi Zhu},
  title = {Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry},
  journal = {Science Journal of Analytical Chemistry},
  volume = {5},
  number = {6},
  pages = {113-118},
  doi = {10.11648/j.sjac.20170506.17},
  url = {https://doi.org/10.11648/j.sjac.20170506.17},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.sjac.20170506.17},
  abstract = {Magnetic solid phase extraction (MSPE) accompanied with fluorescence spectrophotometry using Poly (ionic liquid) immobilized magnetic nanoparticles (PIL-MNPs) as sorbent was introduced for Congo red analysis in food. Poly (1-vinyl-3-butylimidazolium) bromide immobilized (MNPs) were prepared through co-polymerization of 1-vinyl-3-hexylimidazolium-based ionic liquid and vinyl-modified magnetic particles. Some of different types of parameters, such as pH value, adsorption temperature and time, sample volume, eluent type, were studied. Under the optimum conditions, the preconcentration factor for AR was 27. The linear range, detection limit (DL), correlation coefficient (R) and relative standard deviation (RSD) were found to be 0.10-9.00μg/mL, 5.2μg/L, 0.9987 and 3.10% (n=3, c=4.00μg/mL). This method had been successfully applied to the separation / analysis of Congo red in real samples.},
 year = {2018}
}

Copy | Download

TY  - JOUR
T1  - Separation/Analysis of Congo Red by Using Poly (Ionic Liquid) Immobilized Magnetic Nanoparticles Magnetic Solid Phase Extraction Coupled with Fluorescence Spectrophotometry
AU  - Almojtaba Abd Alkhalig Ahmed Bakheet
AU  - Xiashi Zhu
Y1  - 2018/01/02
PY  - 2018
N1  - https://doi.org/10.11648/j.sjac.20170506.17
DO  - 10.11648/j.sjac.20170506.17
T2  - Science Journal of Analytical Chemistry
JF  - Science Journal of Analytical Chemistry
JO  - Science Journal of Analytical Chemistry
SP  - 113
EP  - 118
PB  - Science Publishing Group
SN  - 2376-8053
UR  - https://doi.org/10.11648/j.sjac.20170506.17
AB  - Magnetic solid phase extraction (MSPE) accompanied with fluorescence spectrophotometry using Poly (ionic liquid) immobilized magnetic nanoparticles (PIL-MNPs) as sorbent was introduced for Congo red analysis in food. Poly (1-vinyl-3-butylimidazolium) bromide immobilized (MNPs) were prepared through co-polymerization of 1-vinyl-3-hexylimidazolium-based ionic liquid and vinyl-modified magnetic particles. Some of different types of parameters, such as pH value, adsorption temperature and time, sample volume, eluent type, were studied. Under the optimum conditions, the preconcentration factor for AR was 27. The linear range, detection limit (DL), correlation coefficient (R) and relative standard deviation (RSD) were found to be 0.10-9.00μg/mL, 5.2μg/L, 0.9987 and 3.10% (n=3, c=4.00μg/mL). This method had been successfully applied to the separation / analysis of Congo red in real samples.
VL  - 5
IS  - 6
ER  -

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